Articles | Volume 7, issue 12
https://doi.org/10.5194/amt-7-4417-2014
© Author(s) 2014. This work is distributed under
the Creative Commons Attribution 3.0 License.
the Creative Commons Attribution 3.0 License.
https://doi.org/10.5194/amt-7-4417-2014
© Author(s) 2014. This work is distributed under
the Creative Commons Attribution 3.0 License.
the Creative Commons Attribution 3.0 License.
Research article
| 
12 Dec 2014
Research article |
| 12 Dec 2014
Online derivatization for hourly measurements of gas- and particle-phase semi-volatile oxygenated organic compounds by thermal desorption aerosol gas chromatography (SV-TAG)
G. Isaacman
CORRESPONDING AUTHOR
Department of Environmental Science, Policy, and Management, University of California, Berkeley, CA, USA
N. M. Kreisberg
Aerosol Dynamics Inc., Berkeley, CA, USA
L. D. Yee
Department of Environmental Science, Policy, and Management, University of California, Berkeley, CA, USA
D. R. Worton
Aerosol Dynamics Inc., Berkeley, CA, USA
Department of Environmental Science, Policy, and Management, University of California, Berkeley, CA, USA
A. W. H. Chan
now at: Department of Chemical Engineering and Applied Chemistry, University of Toronto, Toronto, Canada
Department of Environmental Science, Policy, and Management, University of California, Berkeley, CA, USA
J. A. Moss
Department of Environmental Science, Policy, and Management, University of California, Berkeley, CA, USA
S. V. Hering
Aerosol Dynamics Inc., Berkeley, CA, USA
A. H. Goldstein
Department of Civil and Environmental Engineering, University of California, Berkeley, CA, USA
Department of Environmental Science, Policy, and Management, University of California, Berkeley, CA, USA
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- Composition, concentration, and oxidant reactivity of sesquiterpenes in the southeastern U.S. G. Frazier et al. 10.1039/D2EA00059H
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- Development of an in situ dual-channel thermal desorption gas chromatography instrument for consistent quantification of volatile, intermediate-volatility and semivolatile organic compounds R. Wernis et al. 10.5194/amt-14-6533-2021
- Recent advances in mass spectrometry techniques for atmospheric chemistry research on molecular‐level W. Zhang et al. 10.1002/mas.21857
- Synthesis of the Southeast Atmosphere Studies: Investigating Fundamental Atmospheric Chemistry Questions A. Carlton et al. 10.1175/BAMS-D-16-0048.1
- Recent advances in understanding secondary organic aerosol: Implications for global climate forcing M. Shrivastava et al. 10.1002/2016RG000540
- Secondary organic aerosol formation from ambient air in an oxidation flow reactor in central Amazonia B. Palm et al. 10.5194/acp-18-467-2018
- Online Aerosol Chemical Characterization by Extractive Electrospray Ionization–Ultrahigh-Resolution Mass Spectrometry (EESI-Orbitrap) C. Lee et al. 10.1021/acs.est.9b07090
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- Ch3MS-RF: a random forest model for chemical characterization and improved quantification of unidentified atmospheric organics detected by chromatography–mass spectrometry techniques E. Franklin et al. 10.5194/amt-15-3779-2022
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- Coupling a gas chromatograph simultaneously to a flame ionization detector and chemical ionization mass spectrometer for isomer-resolved measurements of particle-phase organic compounds C. Bi et al. 10.5194/amt-14-3895-2021
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- Bulk and molecular-level characterization of laboratory-aged biomass burning organic aerosol from oak leaf and heartwood fuels C. Fortenberry et al. 10.5194/acp-18-2199-2018
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- Ambient Gas-Particle Partitioning of Tracers for Biogenic Oxidation G. Isaacman-VanWertz et al. 10.1021/acs.est.6b01674
- Improving thermal desorption aerosol gas chromatography using a dual-trap design H. Ren et al. 10.1016/j.chroma.2019.04.045
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- Gas–Particle Partitioning of Semivolatile Organic Compounds in a Residence: Influence of Particles from Candles, Cooking, and Outdoors K. Kristensen et al. 10.1021/acs.est.2c07172
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- Analysis of indoor particles and gases and their evolution with natural ventilation C. Fortenberry et al. 10.1111/ina.12584
- Comparative Assessment of Cooking Emission Contributions to Urban Organic Aerosol Using Online Molecular Tracers and Aerosol Mass Spectrometry Measurements D. Huang et al. 10.1021/acs.est.1c03280
- Field intercomparison of the gas/particle partitioning of oxygenated organics during the Southern Oxidant and Aerosol Study (SOAS) in 2013 S. Thompson et al. 10.1080/02786826.2016.1254719
- Infrared Ion Spectroscopy of Environmental Organic Mixtures: Probing the Composition of α-Pinene Secondary Organic Aerosol E. Walhout et al. 10.1021/acs.est.9b02077
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- Comparison of three aerosol chemical characterization techniques utilizing PTR-ToF-MS: a study on freshly formed and aged biogenic SOA G. Gkatzelis et al. 10.5194/amt-11-1481-2018
- An extractive electrospray ionization time-of-flight mass spectrometer (EESI-TOF) for online measurement of atmospheric aerosol particles F. Lopez-Hilfiker et al. 10.5194/amt-12-4867-2019
- Development of a volatility and polarity separator (VAPS) for volatility- and polarity-resolved organic aerosol measurement R. Martinez et al. 10.1080/02786826.2016.1147645
- Analytical methodologies for oxidized organic compounds in the atmosphere A. Tiusanen et al. 10.1039/D3EM00163F
- On the implications of aerosol liquid water and phase separation for organic aerosol mass H. Pye et al. 10.5194/acp-17-343-2017
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- Development of a hydrophilic interaction liquid chromatography (HILIC) method for the chemical characterization of water-soluble isoprene epoxydiol (IEPOX)-derived secondary organic aerosol T. Cui et al. 10.1039/C8EM00308D
- Performance of a new coaxial ion–molecule reaction region for low-pressure chemical ionization mass spectrometry with reduced instrument wall interactions B. Palm et al. 10.5194/amt-12-5829-2019
- Characterizing PM2.5 Emissions and Temporal Evolution of Organic Composition from Incense Burning in a California Residence J. Ofodile et al. 10.1021/acs.est.3c08904
- The chemical assessment of surfaces and air (CASA) study: using chemical and physical perturbations in a test house to investigate indoor processes D. Farmer et al. 10.1039/D4EM00209A
- Automated single-ion peak fitting as an efficient approach for analyzing complex chromatographic data G. Isaacman-VanWertz et al. 10.1016/j.chroma.2017.11.005
- The fuel of atmospheric chemistry: Toward a complete description of reactive organic carbon C. Heald & J. Kroll 10.1126/sciadv.aay8967
- Molecular Composition and Volatility of Organic Aerosol in the Southeastern U.S.: Implications for IEPOX Derived SOA F. Lopez-Hilfiker et al. 10.1021/acs.est.5b04769
- Surface Emissions Modulate Indoor SVOC Concentrations through Volatility-Dependent Partitioning D. Lunderberg et al. 10.1021/acs.est.0c00966
- Biogenic secondary organic aerosols: A review on formation mechanism, analytical challenges and environmental impacts M. Mahilang et al. 10.1016/j.chemosphere.2020.127771
- A technique for rapid source apportionment applied to ambient organic aerosol measurements from a thermal desorption aerosol gas chromatograph (TAG) Y. Zhang et al. 10.5194/amt-9-5637-2016
- Natural and Anthropogenically Influenced Isoprene Oxidation in Southeastern United States and Central Amazon L. Yee et al. 10.1021/acs.est.0c00805
- Hourly organic tracers-based source apportionment of PM2.5 before and during the Covid-19 lockdown in suburban Shanghai, China: Insights into regional transport influences and response to urban emission reductions S. Wang et al. 10.1016/j.atmosenv.2022.119308
- Hourly measurement of PM2.5-bound nonpolar organic compounds in Shanghai: Characteristics, sources and health risk assessment K. Zhang et al. 10.1016/j.scitotenv.2021.148070
- Influence of the vapor wall loss on the degradation rate constants in chamber experiments of levoglucosan and other biomass burning markers A. Bertrand et al. 10.5194/acp-18-10915-2018
- A review of secondary organic aerosols formation focusing on organosulfates and organic nitrates W. Fan et al. 10.1016/j.jhazmat.2022.128406
- Underestimation of biomass burning contribution to PM2.5 due to its chemical degradation based on hourly measurements of organic tracers: A case study in the Yangtze River Delta (YRD) region, China Q. Li et al. 10.1016/j.scitotenv.2023.162071
- Exploration of oxidative chemistry and secondary organic aerosol formation in the Amazon during the wet season: explicit modeling of the Manaus urban plume with GECKO-A C. Mouchel-Vallon et al. 10.5194/acp-20-5995-2020
- Comprehensive detection of analytes in large chromatographic datasets by coupling factor analysis with a decision tree S. Kim et al. 10.5194/amt-15-5061-2022
- Coupling Filter-Based Thermal Desorption Chemical Ionization Mass Spectrometry with Liquid Chromatography/Electrospray Ionization Mass Spectrometry for Molecular Analysis of Secondary Organic Aerosol Y. Huang et al. 10.1021/acs.est.0c01779
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Latest update: 13 Dec 2024
Short summary
We present here a new in situ instrument for ambient measurements of highly polar organic semi-volatile and low-volatility compounds in both the gas and particle phase by gas chromatography. Compounds previously measured only through filter collection and offline analysis can now be measured hourly with, in most cases, less than 20% uncertainty. This instrument provides unprecedented time resolution and the first ever observations of gas-particle partitioning for most of these compounds.
We present here a new in situ instrument for ambient measurements of highly polar organic...
