Articles | Volume 13, issue 5
https://doi.org/10.5194/amt-13-2797-2020
© Author(s) 2020. This work is distributed under
the Creative Commons Attribution 4.0 License.
the Creative Commons Attribution 4.0 License.
https://doi.org/10.5194/amt-13-2797-2020
© Author(s) 2020. This work is distributed under
the Creative Commons Attribution 4.0 License.
the Creative Commons Attribution 4.0 License.
Research article
| Highlight paper
| 
28 May 2020
Research article | Highlight paper |
| 28 May 2020
N2O isotopocule measurements using laser spectroscopy: analyzer characterization and intercomparison
Stephen J. Harris
School of Biological, Earth and Environmental Sciences, UNSW Sydney, NSW, Australia
Australian Nuclear Science and Technology Organisation, Lucas Heights, NSW, Australia
Jesper Liisberg
University of Copenhagen, Niels Bohr Institute, Copenhagen, Denmark
Longlong Xia
Karlsruhe Institute of Technology, IMK-IFU, Garmisch-Partenkirchen,
Germany
Empa, Laboratory for Air Pollution/Environmental Technology,
Dübendorf, Switzerland
Kerstin Zeyer
Empa, Laboratory for Air Pollution/Environmental Technology,
Dübendorf, Switzerland
Longfei Yu
Empa, Laboratory for Air Pollution/Environmental Technology,
Dübendorf, Switzerland
Matti Barthel
ETH Zürich, Department of Environmental Systems Science,
Zürich, Switzerland
Benjamin Wolf
Karlsruhe Institute of Technology, IMK-IFU, Garmisch-Partenkirchen,
Germany
Bryce F. J. Kelly
School of Biological, Earth and Environmental Sciences, UNSW Sydney, NSW, Australia
Dioni I. Cendón
Australian Nuclear Science and Technology Organisation, Lucas Heights, NSW, Australia
Thomas Blunier
University of Copenhagen, Niels Bohr Institute, Copenhagen, Denmark
Johan Six
ETH Zürich, Department of Environmental Systems Science,
Zürich, Switzerland
Empa, Laboratory for Air Pollution/Environmental Technology,
Dübendorf, Switzerland
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Cited
20 citations as recorded by crossref.
- MULTICHARME: a modified Chernin-type multi-pass cell designed for IR and THz long-path absorption measurements in the CHARME atmospheric simulation chamber J. Decker et al. 10.5194/amt-15-1201-2022
- Direct Comb Vernier Spectroscopy for Fractional Isotopic Ratio Determinations M. Siciliani de Cumis et al. 10.3390/s21175883
- Photochemical method for removing methane interference for improved gas analysis M. Polat et al. 10.5194/amt-14-8041-2021
- Soil gas probes for monitoring trace gas messengers of microbial activity J. Roscioli et al. 10.1038/s41598-021-86930-8
- Development and verification of a novel isotopic N 2 O measurement technique for discrete static chamber samples using cavity ring‐down spectroscopy C. Bracken et al. 10.1002/rcm.9049
- Low N2O and variable CH4 fluxes from tropical forest soils of the Congo Basin M. Barthel et al. 10.1038/s41467-022-27978-6
- Precision Spectroscopy of Nitrous Oxide Isotopocules with a Cross-Dispersed Spectrometer and a Mid-Infrared Frequency Comb D. Bailey et al. 10.1021/acs.analchem.0c01868
- The influence of tillage and fertilizer on the flux and source of nitrous oxide with reference to atmospheric variation using laser spectroscopy P. Ostrom et al. 10.1007/s10533-020-00742-y
- A field system for measuring plant and soil carbon fluxes using stable isotope methods C. McCloskey et al. 10.1111/ejss.13016
- Primings of soil organic matter and denitrification mediate the effects of moisture on nitrous oxide production S. Thilakarathna & G. Hernandez-Ramirez 10.1016/j.soilbio.2021.108166
- Global Research Alliance N 2 O chamber methodology guidelines: Considerations for automated flux measurement P. Grace et al. 10.1002/jeq2.20124
- Ideas and perspectives: A strategic assessment of methane and nitrous oxide measurements in the marine environment S. Wilson et al. 10.5194/bg-17-5809-2020
- An approach for calibrating laser‐based N 2 O isotopic analyzers for soil biogeochemistry research E. Stuchiner et al. 10.1002/rcm.8978
- Tracing N2O formation in full-scale wastewater treatment with natural abundance isotopes indicates control by organic substrate and process settings W. Gruber et al. 10.1016/j.wroa.2022.100130
- What can we learn from N 2 O isotope data? – Analytics, processes and modelling L. Yu et al. 10.1002/rcm.8858
- Simultaneous measurement of <i>δ</i><sup>13</sup>C, <i>δ</i><sup>18</sup>O and <i>δ</i><sup>17</sup>O of atmospheric CO<sub>2</sub> – performance assessment of a dual-laser absorption spectrometer P. Steur et al. 10.5194/amt-14-4279-2021
- Assessing nitrous oxide (N2O) isotopic analyzer performance for in-field use J. Francis Clar & R. Anex 10.1016/j.agrformet.2022.108855
- Tracing plant–environment interactions from organismal to planetary scales using stable isotopes: a mini review J. Jez et al. 10.1042/ETLS20200277
- Characterisation of gas reference materials for underpinning atmospheric measurements of stable isotopes of nitrous oxide R. Hill-Pearce et al. 10.5194/amt-14-5447-2021
- Doppler-free two-photon cavity ring-down spectroscopy of a nitrous oxide ( N2O ) vibrational overtone transition G. Zhao et al. 10.1103/PhysRevA.101.062509
19 citations as recorded by crossref.
- MULTICHARME: a modified Chernin-type multi-pass cell designed for IR and THz long-path absorption measurements in the CHARME atmospheric simulation chamber J. Decker et al. 10.5194/amt-15-1201-2022
- Direct Comb Vernier Spectroscopy for Fractional Isotopic Ratio Determinations M. Siciliani de Cumis et al. 10.3390/s21175883
- Photochemical method for removing methane interference for improved gas analysis M. Polat et al. 10.5194/amt-14-8041-2021
- Soil gas probes for monitoring trace gas messengers of microbial activity J. Roscioli et al. 10.1038/s41598-021-86930-8
- Development and verification of a novel isotopic N 2 O measurement technique for discrete static chamber samples using cavity ring‐down spectroscopy C. Bracken et al. 10.1002/rcm.9049
- Low N2O and variable CH4 fluxes from tropical forest soils of the Congo Basin M. Barthel et al. 10.1038/s41467-022-27978-6
- Precision Spectroscopy of Nitrous Oxide Isotopocules with a Cross-Dispersed Spectrometer and a Mid-Infrared Frequency Comb D. Bailey et al. 10.1021/acs.analchem.0c01868
- The influence of tillage and fertilizer on the flux and source of nitrous oxide with reference to atmospheric variation using laser spectroscopy P. Ostrom et al. 10.1007/s10533-020-00742-y
- A field system for measuring plant and soil carbon fluxes using stable isotope methods C. McCloskey et al. 10.1111/ejss.13016
- Primings of soil organic matter and denitrification mediate the effects of moisture on nitrous oxide production S. Thilakarathna & G. Hernandez-Ramirez 10.1016/j.soilbio.2021.108166
- Global Research Alliance N 2 O chamber methodology guidelines: Considerations for automated flux measurement P. Grace et al. 10.1002/jeq2.20124
- Ideas and perspectives: A strategic assessment of methane and nitrous oxide measurements in the marine environment S. Wilson et al. 10.5194/bg-17-5809-2020
- An approach for calibrating laser‐based N 2 O isotopic analyzers for soil biogeochemistry research E. Stuchiner et al. 10.1002/rcm.8978
- Tracing N2O formation in full-scale wastewater treatment with natural abundance isotopes indicates control by organic substrate and process settings W. Gruber et al. 10.1016/j.wroa.2022.100130
- What can we learn from N 2 O isotope data? – Analytics, processes and modelling L. Yu et al. 10.1002/rcm.8858
- Simultaneous measurement of <i>δ</i><sup>13</sup>C, <i>δ</i><sup>18</sup>O and <i>δ</i><sup>17</sup>O of atmospheric CO<sub>2</sub> – performance assessment of a dual-laser absorption spectrometer P. Steur et al. 10.5194/amt-14-4279-2021
- Assessing nitrous oxide (N2O) isotopic analyzer performance for in-field use J. Francis Clar & R. Anex 10.1016/j.agrformet.2022.108855
- Tracing plant–environment interactions from organismal to planetary scales using stable isotopes: a mini review J. Jez et al. 10.1042/ETLS20200277
- Characterisation of gas reference materials for underpinning atmospheric measurements of stable isotopes of nitrous oxide R. Hill-Pearce et al. 10.5194/amt-14-5447-2021
Latest update: 29 Mar 2023
Short summary
The latest commercial laser spectrometers have the potential to revolutionize N2O isotope analysis. However, to do so, they must be able to produce trustworthy data. Here, we test the performance of widely used laser spectrometers for ambient air applications and identify instrument-specific dependencies on gas matrix and trace gas concentrations. We then provide a calibration workflow to facilitate the operation of these instruments in order to generate reproducible and accurate data.
The latest commercial laser spectrometers have the potential to revolutionize N2O isotope...
