Articles | Volume 13, issue 9
https://doi.org/10.5194/amt-13-4773-2020
© Author(s) 2020. This work is distributed under
the Creative Commons Attribution 4.0 License.
the Creative Commons Attribution 4.0 License.
https://doi.org/10.5194/amt-13-4773-2020
© Author(s) 2020. This work is distributed under
the Creative Commons Attribution 4.0 License.
the Creative Commons Attribution 4.0 License.
Research article
| 
09 Sep 2020
Research article |
| 09 Sep 2020
| 09 Sep 2020
Application of TXRF in monitoring trace metals in particulate matter and cloud water
Khanneh Wadinga Fomba
Leibniz Institute for Tropospheric Research (TROPOS), Atmospheric Chemistry Department (ACD), Permoserstraße 15, 04318, Leipzig, Germany
Nabil Deabji
Leibniz Institute for Tropospheric Research (TROPOS), Atmospheric Chemistry Department (ACD), Permoserstraße 15, 04318, Leipzig, Germany
Faculty of Science, Mohammed V University in Rabat, 4 Avenue Ibn Battouta, B.P 1040, 10100 Rabat, Morocco
Sayf El Islam Barcha
Faculty of Science, Mohammed V University in Rabat, 4 Avenue Ibn Battouta, B.P 1040, 10100 Rabat, Morocco
Ibrahim Ouchen
Faculty of Science, Mohammed V University in Rabat, 4 Avenue Ibn Battouta, B.P 1040, 10100 Rabat, Morocco
El Mehdi Elbaramoussi
Faculty of Science, Mohammed V University in Rabat, 4 Avenue Ibn Battouta, B.P 1040, 10100 Rabat, Morocco
Rajaa Cherkaoui El Moursli
Faculty of Science, Mohammed V University in Rabat, 4 Avenue Ibn Battouta, B.P 1040, 10100 Rabat, Morocco
Mimoun Harnafi
Scientific Institute, Mohammed V University in Rabat, Av. Ibn Battouta, B.P 703, 10106 Rabat, Morocco
Souad El Hajjaji
Faculty of Science, Mohammed V University in Rabat, 4 Avenue Ibn Battouta, B.P 1040, 10100 Rabat, Morocco
Abdelwahid Mellouki
Institut de Combustion Aérothermique Réactivité et
Environnement, OSUC-CNRS, 1C Avenue de la Recherche Scientifique, 45071
Orléans CEDEX 2, France
Leibniz Institute for Tropospheric Research (TROPOS), Atmospheric Chemistry Department (ACD), Permoserstraße 15, 04318, Leipzig, Germany
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Cited
30 citations as recorded by crossref.
- Atomic spectrometry update – a review of advances in X-ray fluorescence spectrometry and its special applications C. Vanhoof et al.
- A simple and precise methodology to determine particulate matter mass in atmospheric filters; validation and application cases A. Barba-Lobo et al.
- Multivariate analysis on spatial distribution of chemical elements in river sediment assessed by the total reflection X-ray fluorescence technique I. Dall’Oglio et al.
- Photochemistry of the sea-surface microlayer (SML) influenced by a phytoplankton bloom: a mesocosm study O. Jibaja Valderrama et al.
- Advancement in sensory identification of heavy metal contamination in water: A review on progression from spectroscopic analytical techniques to handheld sensors P. Verma et al.
- Variation of Heavy Metals Accumulation by Malva in Amazonian Ecosystems of Drylands and Floodplains L. Miranda Gomes et al.
- First insights into northern Africa high-altitude background aerosol chemical composition and source influences N. Deabji et al.
- Inhalable Saharan dust induces oxidative stress, NLRP3 inflammasome activation, and inflammatory cytokine release G. Bredeck et al.
- The influence of long-range transported Saharan dust on the inflammatory potency of ambient PM2.5 and PM10 G. Bredeck et al.
- Saharan and Namib Dust Phosphorus Fluxes in the North and South Atlantic Regions K. Fomba et al.
- Insights into tropical cloud chemistry in Réunion (Indian Ocean): results from the BIO-MAÏDO campaign P. Dominutti et al.
- Nasosorption as a Non-Invasive Approach to Measure Metals and Metalloids in the Airway by Benchtop Energy-Dispersive X-Ray Fluorescence K. Adesina et al.
- The seasonal variation of Asian dust, anthropogenic PM, and their sources in Dushanbe, Tajikistan K. Fomba et al.
- A twin site study of size-resolved composition, source apportionment and health impacts of aerosol particles in Morocco N. Deabji et al.
- Method validation and measurement uncertainty estimation in trace element determinations in water samples using total reflection X-rays fluorescence spectrometry L. Chua et al.
- Chemical- and green-precursor-derived carbon dots for photocatalytic degradation of dyes I. Kaur et al.
- Critical review on the development of analytical techniques for the elemental analysis of airborne particulate matter M. Ogrizek et al.
- Assessment of calibration methods for Pb-loaded aerosol filters analysed with X-ray fluorescence under grazing incidence P. Cirelli et al.
- TXRF spectrometry in the bioanalytical sciences: A brief review R. Fernández‐Ruiz
- Reliable compositional analysis of airborne particulate matter beyond the quantification limits of total reflection X-ray fluorescence Y. Kayser et al.
- Novel Hg2+‐Specific “turn-on” fluorescence sensor: Applications in water samples and test strips via real‐time colorimetric assay N. Kaewnok et al.
- Characterisation of temporal and regional differences in the elemental fractionation and mobility of urban particulate matter via online sequential extraction V. Nischwitz et al.
- Particle-bound mercury in Saharan dust-loaded particulate matter in Cabo Verde E. Souza et al.
- Influence of anthropogenic activities on metals, sugars and PAHs in PM10 in the city of Fez, Morocco: Implications on air quality N. Deabji et al.
- Understanding aerosol composition in a tropical inter-Andean valley impacted by agro-industrial and urban emissions L. Mateus-Fontecha et al.
- Atomic spectrometry update – a review of advances in environmental analysis J. Bacon et al.
- Characterization of nebulization generated aerosol particles dispersion and deposition by total reflection X-ray fluorescence D. Ciniglia et al.
- Measurement report: Bio-physicochemistry of tropical clouds at Maïdo (Réunion, Indian Ocean): overview of results from the BIO-MAÏDO campaign M. Leriche et al.
- Elemental analysis of particulate matter by X-ray fluorescence methods: A green approach to air quality monitoring F. Bilo et al.
- Elemental analysis of hourly collected air filters with X-ray fluorescence under grazing incidence H. Takahara et al.
30 citations as recorded by crossref.
- Atomic spectrometry update – a review of advances in X-ray fluorescence spectrometry and its special applications C. Vanhoof et al.
- A simple and precise methodology to determine particulate matter mass in atmospheric filters; validation and application cases A. Barba-Lobo et al.
- Multivariate analysis on spatial distribution of chemical elements in river sediment assessed by the total reflection X-ray fluorescence technique I. Dall’Oglio et al.
- Photochemistry of the sea-surface microlayer (SML) influenced by a phytoplankton bloom: a mesocosm study O. Jibaja Valderrama et al.
- Advancement in sensory identification of heavy metal contamination in water: A review on progression from spectroscopic analytical techniques to handheld sensors P. Verma et al.
- Variation of Heavy Metals Accumulation by Malva in Amazonian Ecosystems of Drylands and Floodplains L. Miranda Gomes et al.
- First insights into northern Africa high-altitude background aerosol chemical composition and source influences N. Deabji et al.
- Inhalable Saharan dust induces oxidative stress, NLRP3 inflammasome activation, and inflammatory cytokine release G. Bredeck et al.
- The influence of long-range transported Saharan dust on the inflammatory potency of ambient PM2.5 and PM10 G. Bredeck et al.
- Saharan and Namib Dust Phosphorus Fluxes in the North and South Atlantic Regions K. Fomba et al.
- Insights into tropical cloud chemistry in Réunion (Indian Ocean): results from the BIO-MAÏDO campaign P. Dominutti et al.
- Nasosorption as a Non-Invasive Approach to Measure Metals and Metalloids in the Airway by Benchtop Energy-Dispersive X-Ray Fluorescence K. Adesina et al.
- The seasonal variation of Asian dust, anthropogenic PM, and their sources in Dushanbe, Tajikistan K. Fomba et al.
- A twin site study of size-resolved composition, source apportionment and health impacts of aerosol particles in Morocco N. Deabji et al.
- Method validation and measurement uncertainty estimation in trace element determinations in water samples using total reflection X-rays fluorescence spectrometry L. Chua et al.
- Chemical- and green-precursor-derived carbon dots for photocatalytic degradation of dyes I. Kaur et al.
- Critical review on the development of analytical techniques for the elemental analysis of airborne particulate matter M. Ogrizek et al.
- Assessment of calibration methods for Pb-loaded aerosol filters analysed with X-ray fluorescence under grazing incidence P. Cirelli et al.
- TXRF spectrometry in the bioanalytical sciences: A brief review R. Fernández‐Ruiz
- Reliable compositional analysis of airborne particulate matter beyond the quantification limits of total reflection X-ray fluorescence Y. Kayser et al.
- Novel Hg2+‐Specific “turn-on” fluorescence sensor: Applications in water samples and test strips via real‐time colorimetric assay N. Kaewnok et al.
- Characterisation of temporal and regional differences in the elemental fractionation and mobility of urban particulate matter via online sequential extraction V. Nischwitz et al.
- Particle-bound mercury in Saharan dust-loaded particulate matter in Cabo Verde E. Souza et al.
- Influence of anthropogenic activities on metals, sugars and PAHs in PM10 in the city of Fez, Morocco: Implications on air quality N. Deabji et al.
- Understanding aerosol composition in a tropical inter-Andean valley impacted by agro-industrial and urban emissions L. Mateus-Fontecha et al.
- Atomic spectrometry update – a review of advances in environmental analysis J. Bacon et al.
- Characterization of nebulization generated aerosol particles dispersion and deposition by total reflection X-ray fluorescence D. Ciniglia et al.
- Measurement report: Bio-physicochemistry of tropical clouds at Maïdo (Réunion, Indian Ocean): overview of results from the BIO-MAÏDO campaign M. Leriche et al.
- Elemental analysis of particulate matter by X-ray fluorescence methods: A green approach to air quality monitoring F. Bilo et al.
- Elemental analysis of hourly collected air filters with X-ray fluorescence under grazing incidence H. Takahara et al.
Saved (final revised paper)
Latest update: 16 May 2026
Short summary
As air quality monitoring networks often sample aerosol particles on quartz filters, the development and applicability of analytical methods with quartz filters are becoming important. In this study different filter preparation methods (e.g., baking, acid digestion) were investigated for quantifying trace metals on quartz and polycarbonate filters, and cloud water using the total reflection X-Ray fluorescence (TXRF) technique, with low detection limits of about 0.3 ng cm−3 for some elements.
As air quality monitoring networks often sample aerosol particles on quartz filters, the...
