Articles | Volume 12, issue 7
https://doi.org/10.5194/amt-12-3503-2019
https://doi.org/10.5194/amt-12-3503-2019
Research article
 | 
02 Jul 2019
Research article |  | 02 Jul 2019

Structural changes of CAST soot during a thermal–optical measurement protocol

Theresa Haller, Christian Rentenberger, Jannik C. Meyer, Laura Felgitsch, Hinrich Grothe, and Regina Hitzenberger

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Latest update: 18 Jun 2024
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Short summary
In thermal–optical measurement techniques – widely used techniques to separate organic and elemental carbon – a filter sample is heated stepwise first in He and then in He+O2. Pyrolysis of organic material occurring during heating in He influences the results but is not fully understood. In this study, structural changes of carbonaceous material during a thermal–optical heating procedure are analyzed with Raman spectroscopy, TEM, UV–VIS and the integrating-sphere method.