Articles | Volume 12, issue 9
https://doi.org/10.5194/amt-12-4965-2019
© Author(s) 2019. This work is distributed under
the Creative Commons Attribution 4.0 License.
the Creative Commons Attribution 4.0 License.
https://doi.org/10.5194/amt-12-4965-2019
© Author(s) 2019. This work is distributed under
the Creative Commons Attribution 4.0 License.
the Creative Commons Attribution 4.0 License.
Research article
| 
13 Sep 2019
Research article |
| 13 Sep 2019
| 13 Sep 2019
Addition of fast gas chromatography to selected ion flow tube mass spectrometry for analysis of individual monoterpenes in mixtures
Michal Lacko
CORRESPONDING AUTHOR
J. Heyrovský Institute of Physical
Chemistry, The Czech Academy of Sciences, Dolejškova 2155/3, 182 23 Prague, Czech Republic
Faculty of Mathematics and Physics, Charles University in Prague, Ke Karlovu 3, 121 16 Prague, Czech Republic
Nijing Wang
Air Chemistry Department, Max-Planck-Institut für Chemie,
Hahn-Meitner-Weg 1, 55128 Mainz, Germany
Kristýna Sovová
J. Heyrovský Institute of Physical
Chemistry, The Czech Academy of Sciences, Dolejškova 2155/3, 182 23 Prague, Czech Republic
Pavel Pásztor
J. Heyrovský Institute of Physical
Chemistry, The Czech Academy of Sciences, Dolejškova 2155/3, 182 23 Prague, Czech Republic
Patrik Španěl
J. Heyrovský Institute of Physical
Chemistry, The Czech Academy of Sciences, Dolejškova 2155/3, 182 23 Prague, Czech Republic
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Cited
13 citations as recorded by crossref.
- Real-Time Volatilomics: A Novel Approach for Analyzing Biological Samples T. Majchrzak et al. 10.1016/j.tplants.2019.12.005
- Hyper-fast gas chromatography and single-photon ionisation time-of-flight mass spectrometry with integrated electrical modulator-based sampling for headspace and online VOC analyses C. Gehm et al. 10.1039/D1AN00114K
- Development of a portable gas chromatography linear ion trap mass spectrometer (GC-LIT-MS) for VOCs analysis in water Q. Junwei et al. 10.1016/j.ijms.2023.117189
- Near real-time quantification of microbial volatile organic compounds from mycoparasitic fungi: Potential for advanced monitoring and pest control F. Lochmann et al. 10.1016/j.jchromb.2024.124237
- Robust Automated SIFT-MS Quantitation of Volatile Compounds in Air Using a Multicomponent Gas Standard V. Langford et al. 10.1021/jasms.3c00312
- Optimization of the determination of volatile organic compounds in plant tissue and soil samples: Untargeted metabolomics of main active compounds N. Kanjana et al. 10.1016/j.mex.2024.102914
- Relative influence of helium and nitrogen carrier gases on analyte ion branching ratios in SIFT-MS P. Španěl et al. 10.1016/j.ijms.2022.116835
- Real-time evaluation of terpene emissions and exposures during the use of scented wax products in residential buildings with PTR-TOF-MS J. Liu et al. 10.1016/j.buildenv.2024.111314
- The peppermint breath test benchmark for PTR-MS and SIFT-MS B. Henderson et al. 10.1088/1752-7163/ac1fcf
- Dynamic aromatics: Evaluating fragrance quality shifts and implementation of real-time rapid detection in Hedychium cut flowers during senescence Y. Zhou et al. 10.1016/j.postharvbio.2024.113193
- Recent developments and applications of selected ion flow tube mass spectrometry (SIFT‐MS) D. Smith et al. 10.1002/mas.21835
- Photoinduced Associative Ionization Time-of-Flight Mass Spectrometry for the Sensitive Determination of Monoterpenes Z. Zhang et al. 10.1080/00032719.2022.2049284
- High-throughput screening for in planta characterization of VOC biosynthetic genes by PTR-ToF-MS M. Li et al. 10.1007/s10265-019-01149-z
12 citations as recorded by crossref.
- Real-Time Volatilomics: A Novel Approach for Analyzing Biological Samples T. Majchrzak et al. 10.1016/j.tplants.2019.12.005
- Hyper-fast gas chromatography and single-photon ionisation time-of-flight mass spectrometry with integrated electrical modulator-based sampling for headspace and online VOC analyses C. Gehm et al. 10.1039/D1AN00114K
- Development of a portable gas chromatography linear ion trap mass spectrometer (GC-LIT-MS) for VOCs analysis in water Q. Junwei et al. 10.1016/j.ijms.2023.117189
- Near real-time quantification of microbial volatile organic compounds from mycoparasitic fungi: Potential for advanced monitoring and pest control F. Lochmann et al. 10.1016/j.jchromb.2024.124237
- Robust Automated SIFT-MS Quantitation of Volatile Compounds in Air Using a Multicomponent Gas Standard V. Langford et al. 10.1021/jasms.3c00312
- Optimization of the determination of volatile organic compounds in plant tissue and soil samples: Untargeted metabolomics of main active compounds N. Kanjana et al. 10.1016/j.mex.2024.102914
- Relative influence of helium and nitrogen carrier gases on analyte ion branching ratios in SIFT-MS P. Španěl et al. 10.1016/j.ijms.2022.116835
- Real-time evaluation of terpene emissions and exposures during the use of scented wax products in residential buildings with PTR-TOF-MS J. Liu et al. 10.1016/j.buildenv.2024.111314
- The peppermint breath test benchmark for PTR-MS and SIFT-MS B. Henderson et al. 10.1088/1752-7163/ac1fcf
- Dynamic aromatics: Evaluating fragrance quality shifts and implementation of real-time rapid detection in Hedychium cut flowers during senescence Y. Zhou et al. 10.1016/j.postharvbio.2024.113193
- Recent developments and applications of selected ion flow tube mass spectrometry (SIFT‐MS) D. Smith et al. 10.1002/mas.21835
- Photoinduced Associative Ionization Time-of-Flight Mass Spectrometry for the Sensitive Determination of Monoterpenes Z. Zhang et al. 10.1080/00032719.2022.2049284
1 citations as recorded by crossref.
Latest update: 06 Mar 2025
Short summary
The soft chemical ionization analytical technique of selected ion flow tube mass spectrometry, SIFT-MS, was enhanced by a fast GC pre-separation unit to identify individual isomers. Experiments were carried out with two GC columns, MXT-1 and MXT-Volatiles, using two reagent ions, H3O+ and NO+, on monoterpene samples (an artificial mixture and coniferous needles). Analyses of product ion ratios allowed for quantification of multiple monoterpenes in partially separated chromatograms.
The soft chemical ionization analytical technique of selected ion flow tube mass spectrometry,...
